Readme created by Shu Xu ------------------- GENERAL INFORMATION ------------------- 1. Title of data set: Supporting data for "Poly(4-ketovalerolactone) from Levulinic acid: Synthesis and Hydrolytic Degradation" 2. Author Information: Principal Investigator Contact Information Name: Thomas R. Hoye Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: hoye@umn.edu ORCID ID: 0000-0001-9318-1477 Associate or Co-investigator Contact Information Name: Shu Xu Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: xuxx0763@umn.edu ORCID ID: 0000-0002-2713-7897 Associate or Co-investigator Contact Information Name: Yuanxian Wang Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: wang4174@umn.edu ORCID ID: 0000-0002-8446-1677 3. Date of data collection (single data, range, approximate date): 2018-2020 4. Geographic location of data collection: All data was collected at the University of Minnesota, Minneapolis, MN. 5. Information about funding sources that supported the collection of the data: Funding for this project was provided by the Center for Sustainable Polymers at the University of Minnesota, a National Science Foundation (NSF)-supported Center for Chemical Innovation (Grant CHE-1901635). -------------------------- SHARING/ACCESS INFORMATION -------------------------- 1. Licenses/restrictions placed on the data: CC0 1.0 Universal 2. Links to publications that cite or use the data: Xu, Shu; Wang, Yuanxian; Hoye, Thomas R. (2020). Poly(4-ketovalerolactone) from Levulinic Acid: Synthesis and Hydrolytic Degradation. Macromolecules, https://doi.org/10.1021/acs.macromol.0c00787 3. Links to other publicly accessible locations of the data: 4. Links/relationships to ancillary data sets: 5. Was data derived from another source? 6. Recommended citation for the data: Xu, Shu; Wang, Yuanxian; Hoye, Thomas R. (2020). Supporting data for Primary data for Poly(4-ketovalerolactone) from Levulinic acid, Synthesis and Hydrolytic Degradation. Retrieved from the Data Repository for the University of Minnesota, https://doi.org/10.13020/jw1d-a958. --------------------- DATA & FILE OVERVIEW --------------------- Purpose Statement: This document describes the sample name convention used and the structure of file format. The document is organized according to the Figures, Tables, and Schemes found in the manuscript and supporting information. General Notes: The folder structure is organized by the order in which each of the figures, tables, and schemes appear in the manuscript and supporting information documents. Data types (i.e. NMR spectra, SEC chromatograms, etc.) are segregated into separate folders. Redundant data - For figures or tables which use data from a previous figure or table, a .txt file using the labeling convention "README - Data for Figure/Table X" has been created, directing the reader to the folder containing the raw data. Files Contained: NMR data: nuclear magnetic resonance (NMR) spectroscopy data is included for each sample. In each folder is the data as downloaded from the instrument. The .fid file can be opened in any NMR analysis software (e.g. MNOVA or iNMR). SEC data: size exclusion chromatography (SEC) data for all of the polymers listed in Tables is included in a single file for each polymer type within each table. Each sample's data is output in two or three columns where the sample name is listed as a header for each column set. The first column shows the elution time in minutes and the second and third columns shows the light scattering or dRI signal, with arbitrary units. All data are saved as a .csv file. DSC data: differential scanning calorimetry (DSC) data is included for the table and figure that used DSC data. The files used to identify Tg's include two columns for each sample, the first is the temperature and the second is heat flow. All data are saved as .csv file. TGA data: Thermogravimetric analysis (TGA) data is included for the table and figure that used TGA data. The files used to identify Td,5%'s include two columns for each sample, the first is the temperature and the second is weight percent. All data are saved as .csv file. ChemDraw: the ChemDraw files for all schemes in the manuscript and supporting information are included as .cdx and .jpg's. Are there multiple versions of the dataset? N -------------------------- METHODOLOGICAL INFORMATION -------------------------- NMR Spectroscopy (NMR): NMR spectra were collected on a Bruker Avance III 500 spectrometer operating at 500 MHz. Chemical shifts were referenced to tetramethylsilane as an internal standard. Differential Scanning Calorimetry (DSC): Differential scanning calorimetry was performed on a TA Instruments Q-1000. Experiments were performed with hermetically sealed aluminum pans. The Tg was estimated as the midpoint of the thermal transition in the curve of the second heating ramp at 10 °C/min, which was calculated using the Trios software. Thermogravimetric Analysis (TGA) – Thermogravimetric analysis was performed on a TA Instruments Q500 Analyzer at 10 °C min-1 to 550 °C under nitrogen atmosphere. Size exclusion chromatography (SEC): Mass-average molar mass, number-average molar mass, and molar mass dispersity was measured using two Agilent 1100 series liquid chromatography instrument. Experiments were performed with three Phenomenex Phenogel-5 columns aligned in series with THF as the mobile phase or three Varian PLgel Mixed C Columns with chloroform as the mobile phase. A Wyatt Technology DAWN DSP MALLS detector and a Wyatt optlab EX RI detector were used to collect the chromatograms for the THF experiments and an HP1047A refractive index detector for the chloroform experiments. The dn/dc values were estimated with an “in-line” method that uses the total area of the RI signal for samples of a known concentration and assumes 100% of the sample mass is recovered. People involved with sample collection, processing, analysis and/or submission: Shu Xu performed all synthesis, collected all NMR data, SEC data, DSC data, and TGA data. Yuanxian Wang performed and optimization of the synthesis of KVL. Folder PATH listing for volume Windows-SSD Volume serial number is B4BF-C19E C:. | listmyfiles.text | README.txt | +---1 - Figure 1 | Figure 1.cdx | Figure 1.jpg | +---10 - Scheme 4 | Scheme 4.cdx | Scheme 4.jpg | +---11 - Data in Supporting Information | +---1 - Table S1 | | | Table S1 scheme.cdx | | | Table S1 scheme.jpg | | | | | \---Table S1 - H NMR spectra | | +---entry 1 - urea | | | \---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---entry 2 - dimethylurea | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5032 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---entry 3 - monomethylurea | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram24064 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---entry 4 - thiourea | | | \---4 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---entry 5 - lutidine | | | \---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---entry 6 - pyridine | | | \---2 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---entry 7 - proline | | \---3 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---10 - Figure S5 | | PKVL TGA.csv | | | +---11 - Figure S6 | | README - data for Figure S6.txt | | | +---12 - Figure S7 | | PAPL TGA.csv | | | +---13 - Figure S8 | | PAPL DSC.csv | | | +---14 - Figure S9 | | PAPL SEC.csv | | | +---15 - Figure S10 | | README - data for Figure S10.txt | | | +---16 - Figure S11 | | 25% KVL TGA.csv | | 50% KVL TGA.csv | | 75% KVL TGA.csv | | 90% KVL TGA.csv | | | +---17 - Figure S12 | | 25% KVL SEC.csv | | | +---18 - Figure S13 | | IR pkvl-co-pvl.png | | | +---19 - Figure S14 | | | Figure S14.cdx | | | Figure S14.jpg | | | | | \---Figure S14 - H NMR spectra | | +---120 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6160 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---60 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6160 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---KVL dmso | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---2 - Figure S1 | | README - data for Figure S1.txt | | | +---20 - Figure S15 | | | Figure S15.cdx | | | Figure S15.jpg | | | | | \---Figure S15 - H NMR spectra | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---KVL dmso | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---21 - Figure S16 | | | Figure S16.cdx | | | Figure S16.jpg | | | | | \---Figure S16 - H NMR spectra | | +---1 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6160 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---30 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---6 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---HLA | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6160 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---PKVL dmso | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---22 - Figure S17 | | | Figure S17.cdx | | | Figure S17.jpg | | | | | \---Figure S17 - H NMR spectra | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---HLA- | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---PKVL dmso | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---23 - Figure S18 | | | Figure S18.cdx | | | Figure S18.jpg | | | | | \---Figure S18 - H NMR spectra | | | README - data for Figure S18.txt | | | | | +---2 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6160 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---24 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6111 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---30 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---4 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---7 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---8 h | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram6160 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---24 - Figure S19 | | | Figure S19.cdx | | | Figure S19.jpg | | | | | \---Figure S19 - H NMR spectra | | +---1 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---1 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---28 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---7 d | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---25 - Figure S20 | | | Figure S20.cdx | | | Figure S20.jpg | | | | | \---Figure S20 - H NMR spectra | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---VL | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---26 - Figure S21 | | | Figure S21.cdx | | | Figure S21.jpg | | | | | \---Figure S21 - H NMR spectra | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---VL | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---27 - Figure S22 | | | Figure S22.cdx | | | Figure S22.jpg | | | | | \---Figure S22 - H NMR spectra | | +---0.5 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---1 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---1 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5011 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---3 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5011 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---9 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5011 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---HVA | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---PVL | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---28 - Figure S23 | | | Figure S23.cdx | | | Figure S23.jpg | | | | | \---Figure S23 - H NMR spectra | | +---15 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---5 min | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | intrng | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---PVL | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---29 - Figure S24 | | | Figure S24.cdx | | | Figure S24.jpg | | | | | \---Figure S24 - H NMR spectra | | +---1 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22288 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---1 w | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22288 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22288 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---4 w | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---8 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22288 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---HVA- | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---3 - Table S2 | | \---Table S2 - H NMR spectra | | +---0.67 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---1.5 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---16 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2.5 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---24 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---48 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram11772 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---6 h | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram11772 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---30 - Table S6 | | README - data for Table S6.txt | | | +---31 - Figure S25 | | | Figure S25.cdx | | | Figure S25.jpg | | | | | \---Figure S25 - H NMR spectra | | +---0.25 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---10 h | | | \---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---2 h | | | \---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---24 h | | | \---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---5 h | | \---1 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---32 - Table S7 | | README - data for Table S7.txt | | | +---33 - Figure S26 | | | Figure S26.cdx | | | Figure S26.jpg | | | | | \---Figure S26 - H NMR spectra | | +---10 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram16626 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---24 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---48 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---5 h | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram16626 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---34 - Table S8 | | README - data for Table S8.txt | | | +---35 - Figure S27 | | Figure S27.cdx | | Figure S27.jpg | | | +---36 - Figure S28 | | | Figure S28.cdx | | | Figure S28.jpg | | | | | \---Figure S28 - H NMR spectra | | | README - data for Figure S28.txt | | | | | +---b. CDCl3 TFA | | | \---2 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---c. CDCl3 HFIP | | \---1 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---37 - NMR spectra | | +---3-HLADL | | | +---3-HLADL C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | spnam5 | | | | | spnam8 | | | | | stanprogram12574 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---3-HLADL H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram12574 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---5-HLADL | | | +---5-HLADL C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | spnam5 | | | | | spnam8 | | | | | stanprogram1545 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---5-HLADL H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram1545 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---APL | | | +---APL C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | spnam5 | | | | | spnam8 | | | | | stanprogram5036 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---APL H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5036 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---KVL H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5036 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---PAPL | | | +---PAPL C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | spnam5 | | | | | spnam8 | | | | | stanprogram10001 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | +---PAPL COSY | | | | | acqu | | | | | acqu2 | | | | | acqu2s | | | | | acqus | | | | | audita.txt | | | | | EA | | | | | format.temp | | | | | fq1list | | | | | gpnam1 | | | | | gradient_calib | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | ser | | | | | shimvalues | | | | | specpar | | | | | stanprogram10001 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | curdat2 | | | | outd | | | | proc | | | | proc2 | | | | proc2s | | | | procs | | | | title | | | | | | | +---PAPL DOSY | | | | +---1 | | | | | | acqu | | | | | | acqus | | | | | | audita.txt | | | | | | fid | | | | | | format.ased | | | | | | format.temp | | | | | | fq1list | | | | | | precom.output | | | | | | pulseprogram | | | | | | scon2 | | | | | | shimvalues | | | | | | specpar | | | | | | uxnmr.info | | | | | | uxnmr.par | | | | | | vtc_pid_settings | | | | | | | | | | | \---pdata | | | | | \---1 | | | | | 1i | | | | | 1r | | | | | auditp.txt | | | | | outd | | | | | proc | | | | | procs | | | | | thumb.png | | | | | title | | | | | | | | | +---2 | | | | | | acqu | | | | | | acqus | | | | | | audita.txt | | | | | | fid | | | | | | format.ased | | | | | | format.temp | | | | | | popt.array | | | | | | popt.protocol | | | | | | popt.protocol.998 | | | | | | popt.protocol.999 | | | | | | pulseprogram | | | | | | scon2 | | | | | | shimvalues | | | | | | specpar | | | | | | uxnmr.info | | | | | | uxnmr.par | | | | | | vtc_pid_settings | | | | | | | | | | | \---pdata | | | | | +---1 | | | | | | 1i | | | | | | 1r | | | | | | auditp.txt | | | | | | outd | | | | | | proc | | | | | | procs | | | | | | thumb.png | | | | | | title | | | | | | | | | | | +---998 | | | | | | 1i | | | | | | 1r | | | | | | auditp.txt | | | | | | outd | | | | | | proc | | | | | | procs | | | | | | thumb.png | | | | | | title | | | | | | used_from | | | | | | | | | | | \---999 | | | | | 1i | | | | | 1r | | | | | auditp.txt | | | | | outd | | | | | proc | | | | | procs | | | | | thumb.png | | | | | title | | | | | used_from | | | | | | | | | +---3 | | | | | | acqu | | | | | | acqus | | | | | | audita.txt | | | | | | fid | | | | | | format.ased | | | | | | format.temp | | | | | | pulseprogram | | | | | | scon2 | | | | | | shimvalues | | | | | | specpar | | | | | | uxnmr.info | | | | | | uxnmr.par | | | | | | vtc_pid_settings | | | | | | | | | | | \---pdata | | | | | \---1 | | | | | 1i | | | | | 1r | | | | | auditp.txt | | | | | outd | | | | | proc | | | | | procs | | | | | thumb.png | | | | | title | | | | | | | | | +---4 | | | | | | acqu | | | | | | acqus | | | | | | audita.txt | | | | | | EA | | | | | | fid | | | | | | format.ased | | | | | | format.temp | | | | | | gpnam6 | | | | | | gpnam7 | | | | | | gpnam8 | | | | | | gradient_calib | | | | | | pulseprogram | | | | | | scon2 | | | | | | shimvalues | | | | | | specpar | | | | | | uxnmr.info | | | | | | uxnmr.par | | | | | | vtc_pid_settings | | | | | | | | | | | \---pdata | | | | | \---1 | | | | | 1i | | | | | 1r | | | | | auditp.txt | | | | | outd | | | | | proc | | | | | procs | | | | | thumb.png | | | | | title | | | | | | | | | +---5 | | | | | | acqu | | | | | | acqus | | | | | | audita.txt | | | | | | EA | | | | | | fid | | | | | | format.ased | | | | | | format.temp | | | | | | gpnam6 | | | | | | gpnam7 | | | | | | gpnam8 | | | | | | gradient_calib | | | | | | pulseprogram | | | | | | scon2 | | | | | | shimvalues | | | | | | specpar | | | | | | uxnmr.info | | | | | | uxnmr.par | | | | | | vtc_pid_settings | | | | | | | | | | | \---pdata | | | | | \---1 | | | | | 1i | | | | | 1r | | | | | assocs | | | | | auditp.txt | | | | | outd | | | | | proc | | | | | procs | | | | | thumb.png | | | | | title | | | | | | | | | \---6 | | | | | acqu | | | | | acqu2 | | | | | acqu2s | | | | | acqus | | | | | audita.txt | | | | | difflist | | | | | Difframp | | | | | EA | | | | | format.ased | | | | | format.temp | | | | | gpnam6 | | | | | gpnam7 | | | | | gpnam8 | | | | | gradient_calib | | | | | pulseprogram | | | | | scon2 | | | | | ser | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | dosy | | | | outd | | | | proc | | | | proc2 | | | | proc2s | | | | procs | | | | t1par | | | | thumb.png | | | | title | | | | | | | +---PAPL H | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram10001 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | +---PAPL HMBC | | | | | acqu | | | | | acqu2 | | | | | acqu2s | | | | | acqus | | | | | audita.txt | | | | | EA | | | | | format.temp | | | | | fq1list | | | | | gpnam1 | | | | | gpnam2 | | | | | gpnam3 | | | | | gradient_calib | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | ser | | | | | shimvalues | | | | | specpar | | | | | stanprogram10001 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | curdat2 | | | | outd | | | | proc | | | | proc2 | | | | proc2s | | | | procs | | | | title | | | | | | | \---PAPL HSQC | | | | acqu | | | | acqu2 | | | | acqu2s | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | EA | | | | format.temp | | | | fq1list | | | | gpnam1 | | | | gpnam2 | | | | gpnam3 | | | | gpnam4 | | | | gradient_calib | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | ser | | | | shimvalues | | | | specpar | | | | spnam14 | | | | spnam18 | | | | spnam3 | | | | spnam31 | | | | spnam7 | | | | stanprogram10001 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | curdat2 | | | outd | | | proc | | | proc2 | | | proc2s | | | procs | | | title | | | | | +---PKVL C | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | spnam5 | | | | spnam8 | | | | stanprogram10929 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---PKVL-co-PVL | | +---PKVL-co-PVL C | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | spnam5 | | | | spnam8 | | | | stanprogram16626 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---PKVL-co-PVL H | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram16626 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---4 - Table S3 | | \---Table S3 - H NMR | | +---T = 23 10 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---T = 23 11 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---T = 41 10 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram21418 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---T = 41 11 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---T = 58 10 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---T = 58 11 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---T = 87 10 d | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---T = 87 11 d | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---5 - Figure S2 | | README - data for Figure S2.txt | | | +---6 - Figure S3 | | | Figure S3.cdx | | | Figure S3.jpg | | | | | \---Figure S3 - H NMR spectra | | +---0.25 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6795 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---1 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6795 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---2 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6795 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---4 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram6795 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---8 h | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram6795 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---7 - Table S4 | | README - data for Table S4.txt | | | +---8 - Figure S4 | | | Figure S4.cdx | | | Figure S4.jpg | | | | | \---Figure S4 - H NMR spectra | | +---0.1 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---0.5 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.ased | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | +---1 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram7583 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---120 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5264 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---16 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram7583 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---168 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5044 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---3 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram7583 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---336 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram10001 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---48 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5264 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---72 h | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram5264 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---8 h | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram7583 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | \---9 - Table S5 | README - data for Table S5.txt | +---2 - Scheme 1 | Schemes 1.cdx | Schemes 1.jpg | +---3 - Table 1 | \---Table 1 - H NMR spectra | +---entry 1 Mn = 1.7 k | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---entry 2 Mn = 3.3 k | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---entry 3 Mn = 5.5 k | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram16626 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---entry 4 Mn = 3.5 k | | \---1 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---entry 5 Mn = 1.2 k | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram5137 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---entry 6 Mn = 2.0 k | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram5036 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | \---entry 7 Sn(II) | \---1 | | acqu | | acqus | | audita.txt | | fid | | format.ased | | format.temp | | fq1list | | precom.output | | pulseprogram | | scon2 | | shimvalues | | specpar | | uxnmr.info | | uxnmr.par | | vtc_pid_settings | | | \---pdata | \---1 | 1i | 1r | auditp.txt | outd | proc | procs | thumb.png | title | +---4 - Figure 2 | Figure 2.cdx | Figure 2.jpg | PKVL DSC.csv | +---5 - Table 2 | | 25% KVL SEC.csv | | Table 2 Scheme.cdx | | Table 2 Scheme.jpg | | | \---Table 2 - H NMR spectra | +---25% KVL | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram16626 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---50% KVL | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram21418 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---75% KVL | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | \---90% KVL | \---10 | | acqu | | acqus | | audita.txt | | fid | | format.temp | | fq1list | | precom.output | | pulseprogram | | scon2 | | shimvalues | | specpar | | uxnmr.info | | uxnmr.par | | vtc_pid_settings | | | \---pdata | \---1 | 1i | 1r | auditp.txt | outd | proc | procs | thumb.png | title | +---6 - Table 3 | 25% KVL DSC.csv | 50% KVL DSC.csv | 75% KVL DSC.csv | 90% KVL DSC.csv | +---7 - Scheme 2 | Schemes 2.cdx | Schemes 2.jpg | +---8 - Figure 3 | | Figure 3 zapf font.cdx | | figure 3.png | | | \---Figure 3 - H NMR spectra | +---entry 1 - KVL | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram5036 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---entry 2 - PKVL | | +---1 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | outd | | | proc | | | procs | | | thumb.png | | | title | | | | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram2194 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---entry 3 - HCl | | \---6 | | | acqu | | | acqus | | | format.ased | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---entry 4 - neutral | | \---30 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | +---entry 5 - Na2CO3 | | \---40 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.ased | | | format.temp | | | fq1list | | | precom.output | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | 1i | | 1r | | auditp.txt | | outd | | proc | | procs | | thumb.png | | title | | | \---entry 6 - NaOH | \---4 | | acqu | | acqus | | audita.txt | | fid | | format.ased | | format.temp | | fq1list | | precom.output | | pulseprogram | | scon2 | | shimvalues | | specpar | | uxnmr.info | | uxnmr.par | | vtc_pid_settings | | | \---pdata | \---1 | 1i | 1r | auditp.txt | outd | proc | procs | thumb.png | title | \---9 - Scheme 3 Scheme 3.cdx Scheme 3.jpg