This file “README_Stepgrowth BG Polymers” was updated on 2020-05-05 by Chris DeRosa ------------------- GENERAL INFORMATION ------------------- Title of Dataset: Supporting Data for “Step-Growth Polyesters with Biobased (R)-1,3-Butanediol” Author Information: Principal Investigator Contact Information Name: Marc A. Hillmyer Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: hillmyer@umn.edu Associate or Co-investigator Contact information Name: Frank S. Bates Institution: University of Minnesota Address: 421 Washington Ave. SE, Minneapolis, MN 55455 Email: bates001@umn.edu Associate or Co-investigator Contact Information Name: Christopher A. DeRosa Institution: University of Minnesota Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: cderosa@umn.edu Associate or Co-investigator Contact Information Name: Xiang Qi Kua Institution: University of Minnesota Address: 207 Pleasant Street SE, Minneapolis, Minnesota 55455 Email: kua00001@umn.edu Date of data collection (August 2018-March 2020): Geographic location of data collection: University of Minnesota Information about funding sources that supported the collection of the data: This research was supported by Genomatica. -------------------------- SHARING/ACCESS INFORMATION -------------------------- 1. Licenses/restrictions placed on the data: CC0 1.0 Universal 2. Links to publications that cite or use the data: DeRosa, C.A., Kua, X.Q., Bates F,S., Hillmyer, M.A. (2020). Step-Growth Polyesters with Biobased (R)-1,3-Butanediol, Industrial & Engineering Chemistry Research. https://doi.org/10.1021/acs.iecr.0c03009 3. Links to other publicly accessible locations of the data: 4. Links/relationships to ancillary data sets: 5. Was data derived from another source? 6. Recommended citation for the data: DeRosa, Christopher A; Kua, Jacelyn; Bates, Frank S; Hillmyer, Marc A. (2020). Step-Growth Polyesters with Biobased (R)-1,3-Butanediol. Retrieved from the Data Repository for the University of Minnesota, https://doi.org/10.13020/7fkh-c288. --------------------- DATA & FILE OVERVIEW --------------------- Purpose Statement: This document describes the raw datasets associated with the manuscript “Step-Growth Polyesters with Biobased (R)-1,3-Butanediol”. General Notes: The files are separated by the type of data, starting with Raw differential Scanning Calorimetry (DSC), Raw Nuclear Magnetic Resonance Spectroscopy (NMR) and so on. Sub folders are separated by the experiment or type of polymers described in the manuscript. In order to understand the names of the files, you will have to have knowledge of the names of the materials and the experiments performed in the manuscript. Files Contained: NMR Spectra: nuclear magnetic resonance (NMR) spectroscopy data is included for each sample as the ouput folders from the Bruker NMR spectroscopy instrument. This contains the .fid, titles and parameters for each sample and can be analyzed by programs such as MNova. DSC data: differential scanning calorimetry (DSC) data is included for the figures that report DSC data. The raw data are provided as .csv files SEC data: size exclusion chromatography (SEC) data for all of the polymers reported in the SI. The raw data are provided as .csv files. Time parameter of the THF-SEC is normalized to a standard. The peaks are normalized to a PS standard; the time columns are different lengths for the dRI and the LS signals. TGA data: Thermogravimetric analysis (TGA) data are included for the Tables that include TGA data. The raw data are provided as .csv files. Copy directory structure. Under each top-level file or folder, add description of the data, file formats, software required to open, and any other information (e.g., conditions, filenaming, weirdness) to help understand and explain the files. Relationship between files: Additional related data collected that was not included in the current data package: Are there multiple versions of the dataset? N -------------------------- METHODOLOGICAL INFORMATION -------------------------- Description of methods used for collection, generation, and processing of data: Methods Nuclear magnetic resonance (NMR) spectra were recorded on a Bruker Advance III HD 400MHz Spectrometer equipped with an autosampler. Chemical shifts are reported in ? units, expressed in ppm using the residual protiochloroform signal (7.26 ppm) as an internal standard. For higher resolution in 13C NMR (101 MHz) spectra to determine polymer microstructure, polymers were concentrated in CDCl3 (~50 mg/mL) and the spectra were recorded with inverse-gated decoupling, a 1.5 second acquisition time and a 2.5-second relaxation delay for a total of 1024 scans. Before size-exclusion chromatography analysis, the polymer was dissolved in the HPLC-grade solvent (THF, CHCl3, or HFIP/TFA) and filtered through a 0.2 nm filter (Whatman) before injection into the column. Size exclusion chromatography (SEC) in THF (1.0 mL/ min at 25 ?) was performed using an Agilent 1260 Infinity series HPLC equipped with a variable-wavelength UV-detector and three sytragel columns (TOSOH). Molecular weights via THF-SEC were determined by conventional calibration vs. polystyrene standards or multi-angle laser light scattering (MALLS: Wyatt HELEOS II) and differential refractive index detectors (Wyatt; Optilab TrEX). The dn/dc values of the polymers in THF (25 ?, 658 nm) were determined using single point-injection, assuming 100% mass recovery of the injected polymer. Size exclusion chromatography in CHCl3 (1.0 mL/ min at 35 ?) was performed using an Agilent 1100 series HPLC equipped with a UV diode-array detector with two styragel columns (Malvern) and the polymer molar masses were determined by conventional calibration versus polystyrene standards. Size exclusion chromatography in hexafluoroisopropanol (HFIP) containing 0.05 M potassium trifluoroacetate (0.35 mL/ min at 40 ?) was performed using a TOSOH EcoSEC Elite HLC-8420 GPC system with two Tosoh TSKgel SuperAWM-H, 9 ?m, mixed-bed columns and the polymer molar masses were determined by conventional calibration versus poly(methyl methacrylate standards). Differential scanning calorimetry (DSC) analyses were performed on a TA Instruments Discovery DSC using hermetically sealed aluminum Tzero pans. Scans were conducted under a nitrogen atmosphere at a heating and cooling rate of 10 ?/min unless otherwise noted. Thermogravimetric analyses (TGA) were performed on a TA Instruments Q500 under nitrogen atmosphere at a heating rate of 10 °C/min. People involved with sample collection, processing, analysis and/or submission: Marc A. Hillmyer facilitated data analysis Frank S. Bates facilitated data analysis Christopher A. DeRosa performed the synthesis and collected the NMR, DSC, and TGA data. Jacelyn Kua performed the synthesis and collected the NMR, DSC, and TGA data. Folder PATH listing for volume OS Volume serial number is B23C-5FFC C:. | listmyfiles.text | print.txt | +---Raw Differential Scanning Calorimetry | +---Biobased Butylene Glycol Polymers | | +---bio-bisBGT | | | first heat cycle_bioBisBGT monomer.csv | | | | | +---Bio-PBGA | | | first cooling cycle_bioPBGA.csv | | | first heating cycle_bioPBGA.csv | | | second heat cycle_bioPBGA.csv | | | | | +---Bio-PBGF | | | first cooling cycle_bioPBGF.csv | | | first heating cycle_bioPBGF.csv | | | second heating cycle_bioPBGF.csv | | | | | +---Bio-PBGS | | | first cooling cycle_bioPBGS.csv | | | first heating cycle_bioPBGS.csv | | | second heating cycle_bioPBGS.csv | | | | | +---Bio-PBGSe | | | first cooling cycle_bioPBGSe.csv | | | first heating cycle_bioPBGSe.csv | | | second heating cycle_bioPBGSe.csv | | | | | +---Bio-PBGSu | | | first cooling cycle_bioPBGSu.csv | | | first heating cycle_bioPBGSu.csv | | | second heating cycle_bioPBGSu.csv | | | | | +---Bio-PBGT | | | first cooling cycle_bioPBGT.csv | | | first heating cycle_bioPBGT.csv | | | second heating cycle_bioPBGT.csv | | | | | +---Bio-PBGTD | | | first cooling cycle_bioPBGTD.csv | | | first heating cycle_bio_PBGTD.csv | | | second heating cycle_bioPBGTD.csv | | | | | +---R-BGBz | | | first heating cycle_RBGz monomer.csv | | | | | \---R-PBGBz | | first cooling cycle_RPBGBz.csv | | first heating cycle_RPBGBz.csv | | second heat cycle_RPBGBz.csv | | | +---Petrol Based Butylene Glycol Polymers | | +---petrol-bisBGT | | | first heating cycle_racemic bisBGT monomer.csv | | | second heating cycle_racemic bisBGT monomer.csv | | | | | +---Petrol-PBGA | | | first cooling cycle_petPBGA.csv | | | first heating cycle_petPBGA.csv | | | second heating cycle_petPBGA.csv | | | | | +---Petrol-PBGF | | | first cooling cycle_petPBGF.csv | | | first heating cycle_petPBGF.csv | | | second heating cycle_petPBGF.csv | | | | | +---Petrol-PBGS | | | first cooling cycle_petPBGS.csv | | | first heating cycle_petPBGS.csv | | | second heating cycle_petPBGS.csv | | | | | +---Petrol-PBGSe | | | first cooling cycle_petPBGSe.csv | | | first heating cycle_petPBGSe.csv | | | second heating cycle_petPBGSe.csv | | | | | +---Petrol-PBGSu | | | first cooling cycle_petPBGSu.csv | | | first heating cycle_petPBGSu.csv | | | second heating cycle_petPBGSu.csv | | | | | +---Petrol-PBGT | | | first cooling cycle_petPBGT.csv | | | first heating cycle_petPBGT.csv | | | second heating cycle_petPBGT.csv | | | | | +---Petrol-PBGTD | | | first cooling cycle_petPBGTD.csv | | | first heating cycle_petPBGTD.csv | | | second heating cycle_petPBGTD.csv | | | | | +---rac-BGBz | | | first heating cycle_racemicBGBz monomer.csv | | | | | \---rac-PBGBz | | first cooling cycle_racemicPBGBz.csv | | first heating cycle_racemicPBGBz.csv | | second heating cycle_racemicPBGBz.csv | | | \---Reference Polymers | +---PBS | | first cooling cycle_PBS.csv | | first heating cycle_PBS.csv | | second heating cycle_PBS.csv | | | +---PMPS | | first cooling cycle_PMPS.csv | | first heating cycle_PMPS.csv | | second heating cycle_PMPS.csv | | | \---PPS | first cooling cycle_PPS.csv | first heating cycle_PPS.csv | second heating cycle_PPS.csv | +---Raw Nuclear Magnetic Resonance Spectroscopy | +---Biobased Butylene Glycol Polymers | | +---bio-bisBGT monomer | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram32139 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Bio-OBGS oligomer | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | +---1H | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | 1i | | | | 1r | | | | auditp.txt | | | | intrng | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | +---DEPT135 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | spnam5 | | | | | stanprogram9678 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | +---HMBC | | | | | acqu | | | | | acqu2 | | | | | acqu2s | | | | | acqus | | | | | audita.txt | | | | | EA | | | | | format.temp | | | | | gpnam1 | | | | | gpnam2 | | | | | gpnam3 | | | | | gradient_calib | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | ser | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | curdat2 | | | | outd | | | | proc | | | | proc2 | | | | proc2s | | | | procs | | | | title | | | | | | | \---HSQC | | | | acqu | | | | acqu2 | | | | acqu2s | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | EA | | | | format.temp | | | | fq1list | | | | gpnam1 | | | | gpnam2 | | | | gpnam3 | | | | gpnam4 | | | | gradient_calib | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | ser | | | | shimvalues | | | | specpar | | | | spnam14 | | | | spnam18 | | | | spnam3 | | | | spnam31 | | | | spnam7 | | | | stanprogram9678 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | proc2 | | | proc2s | | | procs | | | title | | | | | +---bio-PBGA | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1615 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-PBGF | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram13391 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-PBGS | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram21942 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-PBGSe | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Bio-PBGSu | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1265 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-PBGT | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram32139 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-PBGTD | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram11598 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---bio-TsBG | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---R-BGBz | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram11419 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---R-PBGBz | | +---13C | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram32139 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---1H | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram32139 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---Catalyst Screening for Polymerization between Bio-BG and Succinic Acid (1HNMR) | | +---Li(acac) | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Sb2O3 | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | +---mhicad-190621-25 | | | | \---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram12803 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Sn(oct)2 | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---TBD | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Ti(OBu)4 | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Tosic Acid | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---Zn(OAc)2 | | \---1H | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---Petrol based Butlene Glycol Polymers | | +---petro-bisBGT | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram32139 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Petro-PBGA | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1265 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---petro-PBGF | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram21212 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | intrng | | | outd | | | proc | | | procs | | | title | | | | | +---Petro-PBGS | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram21942 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---Petro-PBGSe | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram14057 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram14057 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | 1i | | | 1r | | | auditp.txt | | | intrng | | | outd | | | proc | | | procs | | | title | | | | | +---Petro-PBGSu | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1265 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---petro-PBGT | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram32139 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---rac-BGBz | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram11419 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---rac-PBGBz | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram11419 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---rac-TsBG | | +---13C | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram15569 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---1H | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram15569 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---reference polymers | | +---PBS | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1615 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram1615 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---PMPS | | | +---13C | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | cpdprg2 | | | | | fid | | | | | format.temp | | | | | fq1list | | | | | precom.output | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | stanprogram1615 | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---1H | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram1615 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---PPS | | +---13C | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram1615 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---1H | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | \---Temperature Dependent Kinetics for Bio-BG and Succinic Acid Polymerization (1HNMR) | +---200C | | +---0 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---140 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---180 min | | | +---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---11 | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---190 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---225 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---265 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---300 min | | | +---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---11 | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---360 min | | | +---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---11 | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---40 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---420 min | | | +---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---11 | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---500 min | | | +---10 | | | | | acqu | | | | | acqus | | | | | audita.txt | | | | | fid | | | | | format.temp | | | | | prosol_History | | | | | pulseprogram | | | | | scon2 | | | | | shimvalues | | | | | specpar | | | | | uxnmr.info | | | | | uxnmr.par | | | | | vtc_pid_settings | | | | | | | | | \---pdata | | | | \---1 | | | | outd | | | | proc | | | | procs | | | | title | | | | | | | \---11 | | | | acqu | | | | acqus | | | | audita.txt | | | | cpdprg2 | | | | fid | | | | format.temp | | | | fq1list | | | | precom.output | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | stanprogram22424 | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | +---90 min | | | \---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---Purified Polymer | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | \---240C | +---140 min | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---180 min | | +---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---11 | | | acqu | | | acqus | | | audita.txt | | | cpdprg2 | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram25113 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---190 min | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---210 min | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---235 min | | +---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---11 | | | acqu | | | acqus | | | audita.txt | | | cpdprg2 | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram25113 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---280 min | | +---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---11 | | | acqu | | | acqus | | | audita.txt | | | cpdprg2 | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram25113 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---40 min | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---400 min | | +---10 | | | | acqu | | | | acqus | | | | audita.txt | | | | fid | | | | format.temp | | | | prosol_History | | | | pulseprogram | | | | scon2 | | | | shimvalues | | | | specpar | | | | uxnmr.info | | | | uxnmr.par | | | | vtc_pid_settings | | | | | | | \---pdata | | | \---1 | | | outd | | | proc | | | procs | | | title | | | | | \---11 | | | acqu | | | acqus | | | audita.txt | | | cpdprg2 | | | fid | | | format.temp | | | fq1list | | | precom.output | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | stanprogram25113 | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | +---90 min | | \---10 | | | acqu | | | acqus | | | audita.txt | | | fid | | | format.temp | | | prosol_History | | | pulseprogram | | | scon2 | | | shimvalues | | | specpar | | | uxnmr.info | | | uxnmr.par | | | vtc_pid_settings | | | | | \---pdata | | \---1 | | outd | | proc | | procs | | title | | | \---Purified Polymer | \---10 | | acqu | | acqus | | audita.txt | | fid | | format.temp | | prosol_History | | pulseprogram | | scon2 | | shimvalues | | specpar | | uxnmr.info | | uxnmr.par | | vtc_pid_settings | | | \---pdata | \---1 | outd | proc | procs | title | +---Raw Size Exclusion Chromatography | +---Catalyst Screening for Polymerization between Bio-BG and Succinic Acid (SEC) | | Li(acac).csv | | Sb2O3.csv | | Sn(oct)2.csv | | TBD.csv | | Ti(OBu)4.csv | | TsOH.csv | | Zn(OAc)2.csv | | | +---Purified Polymers | | +---biobased polymers | | | bioPBGA_THF SEC.csv | | | bioPBGF_THF SEC.csv | | | bioPBGSe_THF SEC.csv | | | bioPBGSu_THF SEC.csv | | | bioPBGS_THF SEC.csv | | | bioPBGT_THF SEC.csv | | | RPBGBz_HFIP SEC.csv | | | | | +---petrolbased polymers | | | petPBGA_THF SEC.csv | | | petPBGF_THF SEC.csv | | | petPBGSe_THF SEC.csv | | | petPBGSu_THF SEC.csv | | | petPBGS_THF SEC.csv | | | petPBGT_THF SEC.csv | | | racPBGBz_HFIP SEC.csv | | | | | \---reference polymers | | PBS_CHCl3 SEC.csv | | PMPS_THS SEC.csv | | PPS_THS SEC.csv | | | \---Temperature Dependent Kinetics for Bio-BG and Succinic Acid Polymerization (SEC) | +---200C | | 200C_0min_pre vaccum.csv | | 200C_120 min under vacuum.csv | | 200C_180 min under vacuum.csv | | 200C_20min under vacuum.csv | | 200C_240 min under vacuum.csv | | 200C_300 min under vaucuum.csv | | 200C_50min under vacuum.csv | | 200C_85min under vacuum.csv | | | \---240C | 240C_0 min under vacuum.csv | 240C_10 min under vacuum.csv | 240C_100 min under vacuum.csv | 240C_140 min under vacuum.csv | 240C_240 min under vacuum.csv | 240C_55min under vacuum.csv | 240C_purified Polymer.csv | +---Raw Thermogravimetric Analysis | +---Biobased Butylene Glycol Polymers | | bioPBGA.csv | | bioPBGF.csv | | bioPBGS.csv | | bioPBGSe.csv | | bioPBGSu.csv | | bioPBGT.csv | | bioPBGTD.csv | | RPBGBz.csv | | | +---Petrol based Butylene Glycol Polymers | | petPBGA.csv | | petPBGF.csv | | petPBGS.csv | | petPBGSe.csv | | petPBGSu.csv | | petPBGT.csv | | racPBGBz.csv | | | \---Reference Polymers | PBS.csv | PMPS.csv | PPS.csv | \---Reaction Chemdraw Schemes Polymer Inset_Benzoate Polymers.cdx Polymer Inset_Benzoate Polymers.jpg Scheme 1_Catalyst Screening.cdx Scheme 1_Catalyst Screening.jpg Scheme 2_Synthesis with various diacds.cdx Scheme 2_Synthesis with various diacds.jpg Scheme 3_Sythnesis of terephthalates.cdx Scheme 3_Sythnesis of terephthalates.jpg Scheme 4_Synthesis of benzoate polymers.cdx Scheme 4_Synthesis of benzoate polymers.jpg